Author:
Figgis BN,Raston CL,Sharma RP,White AH
Abstract
The crystal structure of
the title compound, (NH4)2 [FeCl5(H2O)],
has been redetermined by single-crystal X-ray diffraction at 295 K and refined
by full matrix least squares to a residual of 0.054 for 1662 'observed'
reflections. Crystals are orthorhombic, Pnma, a 13.706(2), b 9.924(1), c
7.024(1)Ǻ Z 4. Fe-O is 2.110(4)Ǻ; Fe-Cl range between 2.323(1)Ǻ
(trans to OH2) and 2.350(1)-2.390(1) Ǻ (cis), the latter
distances being very dependent upon hydrogen-bonded interactions with nearby
species.
Cited by
40 articles.
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