Author:
Rae ID,Raston CL,White AH
Abstract
The crystal structure of
N-acetylpiperidine-2-carboxylic acid has been determined by single-crystal
X-ray diffraction methods at 295(1) K and refined by least squares to a
residual of 0.039 for 846 'observed' reflections. Crystals are orthorhombic,
with space group Pbca, a 13.684(6), b 11.602(4), c
11.171(4)Ǻ, Z 8. The ring is a chair structure in which, contrary to an
earlier proposal based on 1H n.m.r. studies, there is almost perfect
staggering about the C(2)-C(3) bond.
Cited by
16 articles.
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