Nonintrusive Analysis of Chemical Agent Identification Sets Using a Portable Fiber-Optic Raman Spectrometer-Reference-Cited by-同舟云学术

Nonintrusive Analysis of Chemical Agent Identification Sets Using a Portable Fiber-Optic Raman Spectrometer

Published:1999-07 Issue:7 Volume:53 Page:850-855
ISSN:0003-7028
Container-title:Applied Spectroscopy
language:en
Short-container-title:Appl Spectrosc

Author:

Christesen Steven¹,Aciver Brian M¹,Procell Lawrence¹,Sorrick David¹,Carrabba Michael¹,Bello Job¹

Affiliation:

1. Research and Technology Directorate, U.S. Army Edgewood Chemical Biological Center, Aberdeen Proving Ground, Maryland 21010 (S.C., B.M., L.P., D.S.); and EIC Laboratories, Inc., Norwood, Massachusetts (M.C., J.B.)

Abstract

A portable fiber-optic Raman system comprising a diode laser, echelle spectrograph, charge-coupled device (CCD) detector, and filtered fiber-optic probe has been used to analyze chemical agents and other toxic chemicals in sealed glass containers. These containers include ampoules and bottles that are contents of chemical agent identification sets (CAIS) developed for use in training military personnel in chemical agent identification, safe handling, and decontamination. Real-time nonintrusive analysis of these sets is required so that the items containing chemical agents can be identified for proper disposal. This paper details the laboratory measurement of Raman spectra of CAIS chemicals, the determination of detection limits for mustard gas and lewisite in chloroform, and the analysis of CAIS items in the field.

Publisher

SAGE Publications

Subject

Spectroscopy,Instrumentation

Link

http://journals.sagepub.com/doi/pdf/10.1366/0003702991947432

Reference7 articles.

1. A New Generation of Raman Instrumentation

2. Raman Spectrometry with Fiber-Optic Sampling

3. Prototype Raman Spectroscopic Sensor for in Situ Mineral Characterization on Planetary Surfaces

4. Marrs T. C., Maynard R. L. and Sidell F. R, Chemical Warfare Agents: Toxicology and Treatment (John Wiley and Sons, Chichester, England, 1996), Chaps. 6–10, pp. 139–227.

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