Colloidal atomic layer deposition on nanocrystals using ligand-modified precursors

Author:

Green Philippe1,Lecina Ona Segura1,Albertini Petru1,Newton Mark2ORCID,Kumar Krishna1,Boulanger Coline1,Leemans Jari3,Thompson Paul4,Loiudice Anna1,Buonsanti Raffaella1ORCID

Affiliation:

1. École polytechnique fédérale de Lausanne

2. ETH

3. EPFL

4. University of Liverpool

Abstract

Abstract

Atomic layer deposition (ALD) is a method to grow thin metal oxide layers on a variety of materials for applications spanning from electronics to catalysis. Extending ALD to colloidally stable nanocrystals promises to combine the benefits of thin metal oxide coatings with the solution processability of nanocrystals. However, challenges persist in applying this method, which relate to finding precursors that promote growth of the metal oxide while preserving colloidal stability throughout the process. Herein, we introduce a colloidal ALD method to coat nanocrystals with amorphous metal oxide shells using metal and oxygen precursors that act as colloidally stabilizing ligands. Our scheme, involves metal-amide precursors modified with solubilizing groups and oleic acid as the oxygen source. The growth of the oxide is self-limiting and proceeds in a layer-by-layer fashion. Our protocol is generalizable and intrinsically scalable. Potential applications in display, light detection and catalysis are envisioned.

Publisher

Research Square Platform LLC

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