Abstract
Abstract
Nanoscale measurement is an essential task of nanomanufacturing, and measurement traceability is a fundamental aspect of nanoscale measurement. High-precision nanoscale measurement instruments (e.g. atomic force microscopes (AFM) and scanning electron microscopes (SEM)) need to be calibrated by traceable standards to ensure their accuracy and reliability. However, due to the suboptimal accuracy, uniformity, and consistency of existing standards, they need to be calibrated by metrological instruments traceable to primary length standards (e.g. physical wavelength standards) before use. This results in a long traceability chain that leads to error accumulation and significantly reduces calibration efficiency. This paper proposes a novel shortened and simplified traceability chain, where the physical wavelength standard corresponding to the 7S3 → 7P4° transition frequency of chromium atoms is materialized into self-traceable gratings using the atom lithography technology. The self-traceable gratings can then be directly applied for calibrating measurement instruments. To verify this approach, the self-traceable gratings are calibrated using a metrological AFM of the Physikalisch-Technische Bundesanstalt. Measurement results confirmed the feasibility of the approach. Particularly, our results show that the self-traceable gratings have excellent uniformity over different measurement areas and consistency over different samples, both at 0.001 nm level. Finally, the application of the self-traceable gratings for the calibrations of a commercial AFM and SEM is demonstrated. The new traceability chain significantly simplifies the calibration process, providing a more reliable and higher efficient calibration approach for advanced nanomanufacturing than that of the state-of-the-art.
Funder
National Key Research and Development Program of China
Special Development Funds for Major Projects of Shanghai Zhangjiang National Independent Innovation Demonstration Zone
National Natural Science Foundation of China
Opening Fund of Shanghai Key Laboratory of Online Detection and Control Technology
Shanghai Science and Technology Commission Young Science and Technology Rising Star Project