Crystal structure of aqua-(5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-κ 4 N,N′,N″,N‴)copper(II) 5-carboxyisophthalate tetrahydrate, C25H50N4CuO11-Reference-Cited by-同舟云学术

Crystal structure of aqua-(5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-κ ⁴ N,N′,N″,N‴)copper(II) 5-carboxyisophthalate tetrahydrate, C₂₅H₅₀N₄CuO₁₁

Published:2023-12-06 Issue:1 Volume:239 Page:11-13
ISSN:1433-7266
Container-title:Zeitschrift für Kristallographie - New Crystal Structures
language:en
Short-container-title:

Author:

Quan Qin-Guo¹,Ou Guang-Chuan¹^ORCID

Affiliation:

1. College of Chemistry and Bioengineering , Hunan University of Science and Engineering , Yongzhou , Hunan 425199 , P.R. China

Abstract

Abstract C25H50N4CuO11, triclinic, P 1 ‾

$\overline{1}$

(no. 2), a = 10.553(6) Å, b = 12.099(7) Å, c = 12.674(8) Å, α = 86.258(6)°, β = 78.131(6)°, γ = 81.408(6)°, V = 1564.8(16) Å3, Z = 2, R gt (F) = 0.0332, wR ref (F 2) = 0.0927, T = 296(2) K.

Publisher

Walter de Gruyter GmbH

Subject

Inorganic Chemistry,Condensed Matter Physics,General Materials Science

Link

https://www.degruyter.com/document/doi/10.1515/ncrs-2023-0405/pdf

Reference8 articles.

1. Bruker. APEX3, SAINT-Plus, XPREP; Bruker AXS Inc.: Madison, Wisconsin, USA, 2016.

2. Sheldrick, G. M. SHELXTL – integrated space-group and crystal-structure determination. Acta Crystallogr. 2015, A71, 3–8.

3. Sheldrick, G. M. Crystal structure refinement with Shelxl. Acta Crystallogr. 2015, C71, 3–8; https://doi.org/10.1107/s2053229614024218.

4. Brandenburg, K. DIAMOND. Visual Crystal Structure Information System. Ver. 4.0; Crystal Impact: Bonn, Germany, 2015.

5. Wang, Q., Ou, G. C. Crystal structure of catena-poly[(5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane)nickel(II)-(κ2-perchlorato)] 3,5-dicarboxybenzoate methanol (1/2), C27H49ClN4NiO12. Z. Kristallogr. N. Cryst. Struct. 2022, 237, 745–747; https://doi.org/10.1515/ncrs-2022-0206.