Crystal structure of catena-poly[(5,5,7,12,12,14-hexamethyl -1,4,8,11-tetraazacyclotetradecane- κ 4 N,N′,Nʺ,N‴)nickel(II)-(μ2-perchlorato-κ 2 O:O′)] 3,5-dicarboxybenzoate – methanol (1/2), C27H49ClN4NiO12-Reference-Cited by-同舟云学术

Crystal structure of catena-poly[(5,5,7,12,12,14-hexamethyl -1,4,8,11-tetraazacyclotetradecane- κ ⁴ N,N′,Nʺ,N‴)nickel(II)-(μ₂-perchlorato-κ ² O:O′)] 3,5-dicarboxybenzoate – methanol (1/2), C₂₇H₄₉ClN₄NiO₁₂

Published:2022-06-10 Issue:4 Volume:237 Page:745-747
ISSN:1433-7266
Container-title:Zeitschrift für Kristallographie - New Crystal Structures
language:en
Short-container-title:

Author:

Wang Qiong¹,Ou Guang-Chuan¹^ORCID

Affiliation:

1. Department of Biology and Chemistry , Hunan University of Science and Engineering , Yongzhou , Hunan , 425199 , P. R. China

Abstract

Abstract C27H49ClN4NiO12, triclinic, P 1 ‾

$\overline{1}$

(no. 2), a = 11.180(2) Å, b = 12.320(3) Å, c = 12.754(3) Å, α = 98.263(2)°, β = 97.524(2)°, γ = 99.470(2)°, V = 1693.1(6) Å3, Z = 2, R gt(F) = 0.0423, wR ref(F 2) = 0.1238, T = 296(2) K.

Publisher

Walter de Gruyter GmbH

Subject

Inorganic Chemistry,Condensed Matter Physics,General Materials Science

Link

https://www.degruyter.com/document/doi/10.1515/ncrs-2022-0206/pdf

Reference7 articles.

1. Bruker. APEX3, SAINT–Plus, XPREP; Bruker AXS Inc.: Madison, Wisconsin, USA, 2016.

2. Sheldrick, G. M. SHELXTL – integrated space-group and crystal-structure determination. Acta Crystallogr. 2015, A71, 3–8; https://doi.org/10.1107/s2053273314026370.

3. Sheldrick, G. M. Crystal structure refinement with SHELXL. Acta Crystallogr. 2015, C71, 3–8; https://doi.org/10.1107/s2053229614024218.

4. Brandenburg, K. DIAMOND. Visual Crystal Structure Information System. Ver. 4.0; Crystal Impact: Bonn, Germany, 2015.

5. Ou, G. C., Yuan, X. Y., Li, Z. Z. catena–poly[(5,5,7,12,12,14- hexamethyl-1,4,8,11-tetraazacyclotetradecane)nickel(II)]-μ-oxido-[dioxidotungstate(VI)]-μ-oxido] tetrahydrate. Acta Crystallogr. 2012, E68, m1173; https://doi.org/10.1107/s1600536812034538.

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