Synthesis and crystal structure of 1-((3R,10S,13R,17S)-10,13-dimethyl-3- (phenylamino)hexadecahydro-1H-cyclopenta[α] phenanthren-17-yl)ethan-1-one, C27H39NO-Reference-Cited by-同舟云学术

Synthesis and crystal structure of 1-((3R,10S,13R,17S)-10,13-dimethyl-3- (phenylamino)hexadecahydro-1H-cyclopenta[α] phenanthren-17-yl)ethan-1-one, C₂₇H₃₉NO

Published:2022-07-07 Issue:5 Volume:237 Page:815-817
ISSN:1433-7266
Container-title:Zeitschrift für Kristallographie - New Crystal Structures
language:en
Short-container-title:

Author:

Zhang Wen-Wen¹^ORCID,Ye Jiang-Hai¹,Zou Juan¹,He Kang¹

Affiliation:

1. Guizhou University of Traditional Chinese Medicine , The Dongqing South Road , Guiyang 550025 , Guizhou Province , P. R. China

Abstract

Abstract C27H39NO, orthorhombic, P212121 (no. 19), a = 10.5248(7) Å, b = 12.6248(7) Å, c = 16.8913(9) Å, V = 2244.4(2) Å3, Z = 4, Rgt (F) = 0.0435, wRref (F 2) = 0.1033, T = 173(2) K.

Publisher

Walter de Gruyter GmbH

Subject

Inorganic Chemistry,Condensed Matter Physics,General Materials Science

Link

https://www.degruyter.com/document/doi/10.1515/ncrs-2022-0266/pdf

Reference13 articles.

1. Dolomanov, O. V., Bourhis, L. J., Gildea, R. J., Howard, J. A. K., Puschmann, H. OLEX2: a complete structure solution, refinement and analysis program. J. Appl. Crystallogr. 2009, 42, 339–341; https://doi.org/10.1107/s0021889808042726.

2. Bruker. APEX2, SAINT and SADABS; Bruker AXS Inc.: Madison, Wisconsin, USA, 2012.

3. Sheldrick, G. M. Crystal structure refinement with SHELXL. Acta Crystallogr. 2015, C71, 3–8; https://doi.org/10.1107/s2053229614024218.

4. Brandenburg, K. DIAMOND. Visual Crystal Structure Information System. Ver. 4.0; Crystal Impact: Bonn, Germany, 2015.

5. Kumar, A., Sati, S. C., Sati, M. D. Chemical and potential biological perspectives of genus Sarcococca (Buxaceae). Nat. Prod. J. 2015, 5, 28–49; https://doi.org/10.2174/2210315505666150219233014.

Cited by 9 articles. 订阅此论文施引文献订阅此论文施引文献，注册后可以免费订阅5篇论文的施引文献，订阅后可以查看论文全部施引文献

1. Synthesis, biological activities and mechanistic studies of C20-ketone pachysandra alkaloids as anti-hepatocellular carcinoma agents;Molecular Diversity;2024-08-19

2. Synthesis and crystal structure of (3E,5S,10S,13S,14S,17Z)-17-ethylidene-10,13-dimethylhexadecahydro-3H-cyclopenta[α]phenanthren-3-one O-(methacryloyl) oxime, C₅₀H₇₄N₂O₄;Zeitschrift für Kristallographie - New Crystal Structures;2023-10-23

3. Synthesis and crystal structure of (3E,5S,10S,13S,14S,17Z)-17-ethylidene-10,13-dimethylhexadecahydro-3H-cyclopenta[α] phenanthren-3-one O-(4-fluorobenzoyl) oxime, C₂₈H₃₆FNO₂;Zeitschrift für Kristallographie - New Crystal Structures;2023-08-07

4. Synthesis and crystal structure of 1-((3R,10S,13S, 17S)-3-((2-methoxyphenyl)amino)-10,13-dimethylhexadecahydro-1H-cyclopenta[α]phenanthren-17-yl)ethan-1-one, C₂₈H₄₁NO₂;Zeitschrift für Kristallographie - New Crystal Structures;2023-05-23

5. Synthesis and crystal structure of 1-((3R,10S,13S,17S)-10,13-dimethyl-3-(m-tolylamino)hexadecahydro-1H-cyclopenta[α]phenanthren-17-yl)ethan-1-one, C₂₈H₄₁NO;Zeitschrift für Kristallographie - New Crystal Structures;2023-04-13