Affiliation:
1. Guizhou University of Traditional Chinese Medicine , Guiyang 550025 , P.R. China
Abstract
Abstract
C28H41NO, triclinic,
P
1
$P1$
(no. 1), a = 6.3144(8) Å, b = 9.7315(13) Å, c = 10.5867(14) Å, α = 111.561(4)°, β =
96.486
(
4
)
∘
$96.486{(4)}^{\circ }$
, γ = 97.128(4)°, V = 591.41(14) Å3, Z = 1,
R
g
t
${R}_{\mathit{g}\mathit{t}}$
(F) = 0.0579,
w
R
r
e
f
$w{R}_{\mathit{r}\mathit{e}\mathit{f}}$
(F
2) = 0.1687, T = 273(2) K.
Subject
Inorganic Chemistry,Condensed Matter Physics,General Materials Science
Reference13 articles.
1. Dolomanov, O. V., Bourhis, L. J., Gildea, R. J., Howard, J. A. K., Puschmann, H. OLEX2: a complete structure solution, refinement and analysis program. J. Appl. Crystallogr. 2009, 42, 339–341; https://doi.org/10.1107/s0021889808042726.
2. Bruker. APEX2, SAINT and SADABS; Bruker AXS Inc.: Madison, Wisconsin, USA, 2012.
3. Sheldrick, G. M. Crystal structure refinement with SHELXL. Acta Crystallogr. 2015, C71, 3–8; https://doi.org/10.1107/s2053229614024218.
4. Brandenburg, K. DIAMOND. Visual Crystal Structure Information System. Ver. 4.0; Crystal Impact: Bonn, Germany, 2015.
5. Kumar, A., Sati, S. C., Sati, M. D., Kumar, S., Singh, D., Bhatt, U., Kaur, G. Chemical and potential biological perspectives of genus Sarcococca (Buxaceae). Nat. Prod. J. 2015, 5, 28–49; https://doi.org/10.2174/2210315505666150219233014.
Cited by
3 articles.
订阅此论文施引文献
订阅此论文施引文献，注册后可以免费订阅5篇论文的施引文献，订阅后可以查看论文全部施引文献
1. Synthesis, biological activities and mechanistic studies of C20-ketone pachysandra alkaloids as anti-hepatocellular carcinoma agents;Molecular Diversity;2024-08-19
2. Synthesis and crystal structure of (3E,5S,10S,13S,14S,17Z)-17-ethylidene-10,13-dimethylhexadecahydro-3H-cyclopenta[α]phenanthren-3-one O-(methacryloyl) oxime, C50H74N2O4;Zeitschrift für Kristallographie - New Crystal Structures;2023-10-23
3. Synthesis and crystal structure of (3E,5S,10S,13S,14S,17Z)-17-ethylidene-10,13-dimethylhexadecahydro-3H-cyclopenta[α] phenanthren-3-one O-(4-fluorobenzoyl) oxime, C28H36FNO2;Zeitschrift für Kristallographie - New Crystal Structures;2023-08-07