Crystal structure of diaqua-bis(μ2-6-phenylpyridine-2-carboxylate-κ3N,O:O)-bis(6-phenylpyridine-2-carboxylato-κ2N,O)lead(II) – N,N-dimethylformamide – water (1/2/4), C54H58N6O16Pb2-Reference-Cited by-同舟云学术

Crystal structure of diaqua-bis(μ2-6-phenylpyridine-2-carboxylate-κ3N,O:O)-bis(6-phenylpyridine-2-carboxylato-κ2N,O)lead(II) – N,N-dimethylformamide – water (1/2/4), C54H58N6O16Pb2

Published:2021-08-13 Issue:6 Volume:236 Page:1199-1201
ISSN:1433-7266
Container-title:Zeitschrift für Kristallographie - New Crystal Structures
language:en
Short-container-title:

Author:

Tai Xi-Shi¹^ORCID,Liang Lei²,Li Xiang-Tao¹,Cao Shu-Hua¹,Wang Li-Hua¹

Affiliation:

1. College of Chemistry and Chemical Engineering, Weifang University , Weifang , Shandong 261061 , P. R. China

2. School of Harbin Light Industry , Harbin , Heilongjiang 150040 , P. R. China

Abstract

Abstract C54H58N6O16Pb2, triclinic, P 1 ‾

$P‾{1}$

(no. 2), a = 9.4690(6) Å, b = 12.9374(6) Å, c = 13.2303(7) Å, V = 1341.90(15) Å3, α = 63.395(5)°, β = 74.291(5)°, γ = 69.113(5)°, Z = 1, R gt (F) = 0.0284, wR ref(F 2) = 0.0484, T = 150 K.

Publisher

Walter de Gruyter GmbH

Subject

Inorganic Chemistry,Condensed Matter Physics,General Materials Science

Link

https://www.degruyter.com/document/doi/10.1515/ncrs-2021-0277/pdf

Reference9 articles.

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3. Sheldrick, G. M. Crystal structure refinement with SHELXL. Acta Crystallogr. 2015, C71, 3–8; https://doi.org/10.1107/s2053229614024218.

4. Brandenburg, K. DIAMOND. Visual Crystal Structure Information System (Ver. 3.2); Crystal Impact: Bonn, Germany, 2012.

5. Wang, H., Han, S., Dun, L.-N., Zhang, B.-S., Chen, X., Wang, J.-J., Li, C.-B., Liu, C.-L. Crystal structure, thermal behavior, luminescence and theoretical calculation of a new Pb(II) coordination complex. J. Mol. Struct. 2020, 1222, 128950; https://doi.org/10.1016/j.molstruc.2020.128950.

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