The crystal structure of tetrakis(6-phenylpyridine-2-carboxylate-κ 2 N,O)-bis(μ2-6-phenylpyridine-2-carboxylate-κ 2 O:O′)-bis(μ2-6-phenylpyridine-2-carboxylate-κ 3N,O:O)tetralead(II) C48H32N4O8Pb2-Reference-Cited by-同舟云学术

The crystal structure of tetrakis(6-phenylpyridine-2-carboxylate-κ ² N,O)-bis(μ₂-6-phenylpyridine-2-carboxylate-κ ² O:O′)-bis(μ₂-6-phenylpyridine-2-carboxylate-κ ³N,O:O)tetralead(II) C₄₈H₃₂N₄O₈Pb₂

Published:2022-09-19 Issue:6 Volume:237 Page:1113-1116
ISSN:1433-7266
Container-title:Zeitschrift für Kristallographie - New Crystal Structures
language:en
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Author:

Li-Hua Wang¹,Hao-Wen Tai²,Qiu-Shi Li³,Yu-Pei Xia¹^ORCID,Xi-Shi Tai¹^ORCID

Affiliation:

1. College of Chemistry and Chemical Engineering , Weifang University , Weifang , Shandong 261061 , P. R. China

2. School of Science and Technology , Hong Kong Metropolitan University , 30 Mok Oi Street, Kowloon District , Hong Kong , P. R. China

3. College of Chemical Engineering , Qingdao University of Science & Technology , Qingdao , Shandong 266042 , P. R. China

Abstract

Abstract C48H32N4O8Pb2, triclinic, P 1 ‾

$P\overline{1}$

(no. 2), a = 9.2712(8) Å, b = 14.5959(13) Å, c = 16.6178(13) Å, α = 76.089(7)°, β = 77.068(7)°, γ = 74.717(7)°, V = 2074.5(3) Å3, Z = 2, R gt (F) = 0.0563, wR ref (F 2) = 0.1783, T = 250 K.

Publisher

Walter de Gruyter GmbH

Subject

Inorganic Chemistry,Condensed Matter Physics,General Materials Science

Link

https://www.degruyter.com/document/doi/10.1515/ncrs-2022-0378/pdf

Reference16 articles.

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3. Sheldrick, G. M. Crystal structure refinement with SHELXL. Acta Cryst. 2015, C71, 3–8; https://doi.org/10.1107/s2053229614024218.

4. Brandenburg, K. DIAMOND. Visual Crystal Structure Information System. Ver. 3.2; Crystal Impact: Bonn, Germany, 2012.

5. Al-Jibori, S. A., Amen, M. M., Alheety, M. A., Karadag, A., Wagner, C. Hydrogen storage capacity of novel mixed ligand complexes of lead(II): molecular structure of [Pb2(tsac)4(μ-dppe)]. Inorg. Chem. Commun. 2021, 125, 108444; https://doi.org/10.1016/j.inoche.2021.108444.

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