Rheological Characterization of Yield-Stress Fluids with Brookfield Viscometer

Author:

Potanin Andrei1,Marron Greggory1

Affiliation:

1. Colgate-Palmolive Co ., 909 River Rd., Piscataway, NJ 08855 , United States of America

Abstract

Abstract This paper analyzes various techniques to use viscometers equipped with vane spindles to characterize rheological properties of yield stress fluids. Specifically, application of Brookfield viscometers to this end is discussed. A wide selection of toothpastes and lotions were tested. It is shown that a simple method based on apparent shear rate and stress, commonly referred to as a representative viscosity method, works well for moderately non-Newtonian samples but may significantly underestimate viscosity for samples with a more pronounced yield stress behavior. To get more accurate data an integral equation relating torque to angular velocity needs to be solved which can be easily done numerically to get a good agreement between the data collected on an inexpensive viscometer and the data from high-end rheometers.

Publisher

Walter de Gruyter GmbH

Subject

Condensed Matter Physics,General Materials Science

Reference22 articles.

1. [1] Brookfield DV2T Viscometer Operating Instructions, Manual 13-167-B0614 or any other for digital viscometer available at brook-fieldengineering.com.

2. [2] Mitschka, P., Simple conversion of Brookfield RVT readings into viscosity functions. Rheologica Acta, 21 (1982) 207-209.

3. [3] Wein, O.P., Mitschka, P., Wichterle, K. Immersional rotational viscometry. A course manual, published (in Czech) in Edice MACRO N-1 by the Institute of Macromolecular Chemistry, Czechoslovak Acd. Sci., Prague (1977)

4. [4] Briggs, J.L., and Steffe, J.F. Using Brookfield Data and the Mitschka Method to Evaluate Power-law Foods. J. Texture Studies. 28 (1997) 517-522.

5. [5] Anderson, V.J, and Meeten, G.H, Interpretation of T-Bar Tool Measurements for Yield Stress Materials. Appl. Rheol. 22 (2012) 55370.

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