Microwave-Assisted Preparation of Activated Carbon from Eupatorium Adenophorum: Effects of Preparation Parameters

Author:

Cheng Song1234,Zhang Shengzhou1234,Zhang Libo1234,Xia Hongying1234,Peng Jinhui1234,Wang Shixing1234

Affiliation:

1. State Key Laboratory of Complex Nonferrous Metal Resources Clean Utilization, Kunming University of Science and Technology, Kunming, Yunnan 650093, China

2. Yunnan Provincial Key Laboratory of Intensification Metallurgy, Kunming University of Science and Technology, Kunming, Yunnan 650093, China

3. National Local Joint Laboratory of Engineering Application of Microwave Energy and Equipment Technology, Kunming, Yunnan 650093, China

4. Faculty of Metallurgical and Energy Engineering, Kunming University of Science and Technology, Kunming, Yunnan 650093, China

Abstract

AbstractEupatorium adenophorum, global exotic weeds, was utilized as feedstock for preparation of activated carbon (AC) via microwave-induced KOH activation. Influences of the three vital process parameters – microwave power, activation time and impregnation ratio (IR) – have been assessed on the adsorption capacity and yield of AC. The process parameters were optimized utilizing the Design Expert software and were identified to be a microwave power of 700 W, an activation time of 15 min and an IR of 4, with the resultant iodine adsorption number and yield being 2,621 mg/g and 28.25 %, respectively. The key parameters that characterize the AC such as the brunauer emmett teller (BET) surface area, total pore volume and average pore diameter were estimated to be 3,918 m2/g, 2,383 ml/g and 2.43 nm, respectively, under the optimized process conditions. The surface characteristics of AC were characterized by Fourier transform infrared spectroscopy, scanning electron microscope and Transmission electron microscope.

Publisher

Walter de Gruyter GmbH

Subject

Physical and Theoretical Chemistry,Mechanics of Materials,Condensed Matter Physics,General Materials Science

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