Regiospecific Carboxylation of Certain Methoxylated 2-Tetralones

Author:

Beres James A.,Cannon Joseph G

Publisher

Informa UK Limited

Subject

Organic Chemistry

Reference5 articles.

1. The Carboxylation and Formylation of Certain 2-Tetralones1,2

2. Synthesis of natural ketols of the pyrethrin series

3. Stiles, M. personal communication, cited by Pelletier, et al., ref. 2

4. 5,6-Dimethoxy-2-tetralone was treated with NaH then with diethyl carbonate according to the procedure in ref. 1. The resulting 1-carbethoxylated 2-tetralone NMR spectrum (CDCl3) showed the following: δ 13.2 (OH); 3.74, 3.80 (s, 6H, OCH3); and a multiplet centered at 2.40 and 2.80 (4H; protons at positions 3 and 4)

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