1. a SERC Daresbury Laboratory , Daresbury , Warrington WA4 4AD, England
2. b Department of Physics , University of Leicester , Leicester , LE1 7RH, England
3. c Department of Physical Chemistry , University of Cambridge , Cambridge , CB2 1EP, England
4. d Department of Chemistry , University of Keele , Keele , Staffordshire ST5 5BG, England
5. e Solid State Division, Oak Ridge National Laboratory , Oak Ridge , Tennessee , 37831 , U.S.A.