On the issues of resolving a low melting combination as a definite eutectic or an elusive cocrystal: A critical evaluation

Author:

CHERUKUVADA SURYANARAYAN

Publisher

Springer Science and Business Media LLC

Subject

General Chemistry

Reference39 articles.

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2. (a) Askeland D R and Fulay P P 2009 In Essentials of Materials Science and Engineering 2nd edn. (Toronto: Cengage Learning); (b) Sharma S D, Kitano H and Sagara K 2004 Res. Rep. Fac. Eng. Mie Univ. 29 31; (c) Lee L-S, Lin C-W and Kao C-H 2000 Ind. Eng. Chem. Res. 39 2068; (d) Urbanus J, Roelands C P M, Verdoes D, Jansens D J and ter Horst J H 2010 Cryst. Growth Des. 10 1171; (e) Bolton O and Matzger A J 2011 Angew. Chem. Int. Ed. 50 8960; (f) Morimoto M and Irie M 2010 J. Am. Chem. Soc. 132 14172; (g) Shilei L, Neng Z and Guohui F 2006 Energy Build. 38 708; (h) Huang X, Qin D, Zhang X, Luo Y, Huang S, Li D and Meng Q 2013 RSC Adv. 3 6922; (i) Griffini G, Brambilla L, Levi M, Castiglioni C, Zoppo M D and Turri S 2014 RSC Adv. 4 9893

3. Although there is no sharp organic/molecular restriction for cocrystals and several ionic cocrystals were known (Beevers C A and Cochran W 1946 Nature 157 872; Braga D, Grepioni F, Maini L, Prosperi S, Gobetto R and Chierotti M R 2010 Chem. Commun. 46 7715), majority of the definitions on cocrystal[1]k state it to be a multi-molecular entity and it had been termed as ‘molecular compound’, ‘molecular complex’, ‘molecular crystal’, ‘heteromolecular crystal’ etc. (Stahly G P 2009 Cryst. Growth Des. 9 4212). Molecular salt and cocrystal as the two extremes of the salt–cocrystal continuum, with the former being the ionized entity and the latter an un-ionized one, were well appreciated in the literature.[1]b,c,o,p

4. The analogy between cocrystal and intermetallic compound brought herein should be considered in a supramolecular/structural sense and not at atomic/ molecular level where the bonding is different. Both cocrystal and intermetallic compound have distinct structural integrity as compared to their respective parent materials.

5. Aitipamula S, Banerjee R, Bansal A K, Biradha K, Cheney M L, Choudhury A R, Desiraju G R, Dikundwar A G, Dubey R, Duggirala N, Ghogale P P, Ghosh S, Goswami P K, Goud N R, Jetti R K R, Karpinski P, Kaushik P, Kumar D, Kumar V, Moulton B, Mukherjee A, Mukherjee G, Myerson A S, Puri V, Ramanan A, Rajamannar T, Reddy C M, Rodríguez-Hornedo N, Rogers R D, Row T N G, Sanphui P, Shan N, Shete G, Singh A, Sun C C, Swift J A, Thaimattam R, Thakur T S, Thaper R K, Thomas S P, Tothadi S, Vangala V R, Vishweshwar P, Weyna D R and Zaworotko M J 2012 Cryst. Growth Des. 12 2147; correction - 2012 12 4290

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