Structural Integrity of a Standpipe Component in a Petrochemical Catalytic Cracking Unit: Part 2—Assessment of Embrittlement Effects

Author:

de O. Bueno Levi1,Marino Luiz1,Serra Flavio A. S.2,Gazini Fernando T.2

Affiliation:

1. Department of Materials Engineering, Universidade Federal Sao Carlos, Rodovia W. Luiz, km.235, 13565-905 Sao Carlos (SP), Brazil

2. PETROBRAS/REPLAN, Rodovia SP 332, km 132, 13.100 Paulinia (SP), Brazil

Abstract

During a shutdown for general maintenance of a catalytic cracking unit, intergranular cracks were observed to occur during welding of the regenerator’s standpipe component manufactured from 2 1/4 Cr-1Mo steel. The cracking was observed to be related to intensive carbide precipitation in grain boundaries. To overcome the problem it was decided to heat-treat the relevant section of the component to dissolve these carbides and make possible its welding to a new virgin section of the tube. Samples of the material in its various conditions (virgin, ex-service, heat-treated, and welded) were taken to check the efficiency of the thermal treatment in reducing the embattlement effects and to carry out a general assessment of the remaining life of the component related to creep behavior considering notched bar creep specimens. [S0094-4289(00)00503-X]

Publisher

ASME International

Subject

Mechanical Engineering,Mechanics of Materials,Condensed Matter Physics,General Materials Science

Reference9 articles.

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3. Nishizaka, Y., Hara, Y., Hori, A., Tsukahara, H., Miyano, K., Wada, T., and Cox, T. B., 1985, “Changes in microstructure and mechanical properties of Cr-Mo reactor vessel steels during long-term service,” ASME J. Pressure Vessel Technol., 107, pp. 285–294.

4. Roe, G. J., and Bramfitt, B. L., 1992, Metals Handbook, 10th edition, “Properties and Selection: Irons, Steels and High-Performance Alloys,” ASM International, 8, pp. 737–754.

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