Affiliation:
1. School of Materials and Chemical Engineering, Anhui Jianzhu University, Hefei, People’s Republic of China
Abstract
The synthesis of C-ring hydrogenated sinomenine derivatives is accomplished from sinomenine by treatment with Zn-Hg/HCl, halogenation with NIS, and Heck reactions with various acrylates. A total of nine novel sinomenine cinnamate derivatives are obtained in 84%–93% yields. The structures of all the derivatives are characterized by 1H NMR, 13C NMR, and MS spectroscopy.
Funder
university natural science research project of anhui province
Science and Technology Innovation Foundation for College Students
Cited by
8 articles.
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