One-pot synthesis of azo compounds in the absence of acidic or alkaline additives-Reference-Cited by-同舟云学术

One-pot synthesis of azo compounds in the absence of acidic or alkaline additives

Published:2020-10-19 Issue: Volume: Page:174751982096418
ISSN:1747-5198
Container-title:Journal of Chemical Research
language:en
Short-container-title:Journal of Chemical Research

Author:

Liu Ting-Ting¹,Yan Jiao-Zhao¹,Cheng Xin-Wang²,Duan Pan¹,Zeng Yao-Fu¹^ORCID

Affiliation:

1. Institute of Pharmacy and Pharmacology, Hunan Provincial Key Laboratory of Tumor Microenvironment Responsive Drug Research, University of South China, Hengyang, PR China

2. People’s Hospital of Xiushan County, Chongqing, PR China

Abstract

A one-pot method for the synthesis of azo compounds by the reaction of β-naphthol with aryl amines using t-BuONO as the nitrosonium source in DCM at room temperature was developed. This method features mild reaction conditions, a simple experimental procedure, and is free of acidic or alkaline additives.

Funder

natural science foundation of hunan province

Hunan Educational Committee

Publisher

SAGE Publications

Subject

General Chemistry

Link

http://journals.sagepub.com/doi/pdf/10.1177/1747519820964182

Reference37 articles.

1. Process intensification in azo dyes

2. Carboxyl and nitrite functionalized graphene quantum dots as a highly active reagent and catalyst for rapid diazotization reaction and synthesis of azo-dyes under solvent-free conditions

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