Effect of sintering parameters on the microstructure and compressive mechanical properties of porous Fe scaffold fabricated using 3D printing and pressure less microwave sintering

Abstract

The demand for the porous scaffold has been increasing globally in the biomedical field due to numerous advantages over dense structures like high damping capacity, high specific strength, and improved cell integration growth. In the present study, porous iron scaffolds were fabricated using micro-extrusion-based three-dimensional printing and pressureless microwave sintering. For the preparation of samples, metal-based polymeric ink was developed. Thereafter, cylindrical samples were printed and then sintered in a microwave sintering furnace. The experimental investigations were performed to estimate the effect of sintering parameters such as sintering temperature, heating rate and soaking time on the compressive and microstructural property of the fabricated samples. Microstructural characterization was done using the electron backscatter diffraction technique. The experimental observations deduced that the compressive yield strength and apparent density of the sintered sample increased with the increase in sintering temperature and decreased with a further rise in temperature. Moreover, the electron backscatter diffraction analysis unveiled that the high heating rate resulted in the reduction of compressive yield strength due to rapid grain growth. Additionally, the significant effect of soaking time on the compressive mechanical properties was also noticed due to the increase in the grain size diameter. From the X-ray diffraction plot, it was found that there was no contamination present in the fabricated scaffold. In order to evaluate the process capability, a case study was performed wherein the topologically ordered porous structure of iron was fabricated at optimum sintering parameters.