Application of High-Performance Liquid Chromatography for Simultaneous Identification of Integristerone A, 20-Hydroxyecdysone, Ecdysone and 2-Deoxy-20-hydroxyecdysone-Reference-Cited by-同舟云学术

Application of High-Performance Liquid Chromatography for Simultaneous Identification of Integristerone A, 20-Hydroxyecdysone, Ecdysone and 2-Deoxy-20-hydroxyecdysone

Published:2007-11 Issue:11 Volume:2 Page:1934578X0700201
ISSN:1934-578X
Container-title:Natural Product Communications
language:en
Short-container-title:Natural Product Communications

Author:

Rybin Viatcheslav¹,Boltenkov Eugene²,Novozhilova Elena³

Affiliation:

1. Pacific Research Fisheries Centre, 4, Shevchenko Alley, Vladivostok, 690950, Russian Federation

2. Botanical Garden-Institute of the Far-Eastern Branch of the Russian Academy of Sciences, 142, Makovskogo St., Vladivostok, 690024, Russian Federation

3. Pacific Institute of Bioorganic Chemistry of the Far-Eastern Branch of the Russian Academy of Sciences, 159, Prospect 100-letiya Vladivostoka, Vladivostok, 690022, Russian Federation

Abstract

Conditions for separation and identification of integristerone A (1), 20-hydroxyecdysone (2), ecdysone (3) and 2-deoxy-20-hydroxyecdysone (4) by reversed-phase HPLC with UV and mass-selective detection at atmospheric pressure chemical ionization have been developed. Correlation between quasi-molecular ions fragmentation and structure peculiarities of the studied ecdysteroids has been shown. Application of these conditions for the analysis of extract from the inflorescences of Serratula komarovii made it possible to reveal and to identify compounds 1, 2 and 4.

Publisher

SAGE Publications

Subject

Complementary and alternative medicine,Plant Science,Drug Discovery,Pharmacology,General Medicine

Link

http://journals.sagepub.com/doi/pdf/10.1177/1934578X0700201110

Reference13 articles.

1. Development of a new high‐performance liquid chromatography‐mass spectrometric method for the analysis of ecdysteroids in biological extracts

2. Purification and characterization of plant ecdysteroids of Silene species

3. ReesHH. (1989) Zooecdysteroids: Structure and occurrence. In Ecdysone: From Chemistry to Mode of Action. KoolmanJ (Ed). Thieme, Stuttgart, 28–38.

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