Isolation and Identification of 2-Phenylethyl Disaccharide Glycosides and Mono Glycosides from Rose Flowers, and Their Potential Role in Scent Formation-Reference-Cited by-同舟云学术

Isolation and Identification of 2-Phenylethyl Disaccharide Glycosides and Mono Glycosides from Rose Flowers, and Their Potential Role in Scent Formation

Published:2001-01 Issue:2 Volume:65 Page:442-445
ISSN:0916-8451
Container-title:Bioscience, Biotechnology, and Biochemistry
language:en
Short-container-title:Bioscience, Biotechnology, and Biochemistry

Author:

WATANABE Shuzo,HASHIMOTO Ikue,HAYASHI Kentaro,YAGI Kensuke,ASAI Tatsuo,KNAPP Holger,STRAUBINGER Markus,WINTERHALTER Peter,WATANABE Naoharu

Publisher

Oxford University Press (OUP)

Subject

Organic Chemistry,Molecular Biology,Applied Microbiology and Biotechnology,General Medicine,Biochemistry,Analytical Chemistry,Biotechnology

Link

http://www.tandfonline.com/doi/pdf/10.1271/bbb.65.442

Reference2 articles.

1. 4) Bureau, S. Ph. D Thesis from University of Montpellier, France (1996).

2. 10) NMR data for 2:1H-NMR (500 MHz, D2O)δ:2.99 (2H, t, J=7.0, H2-7), 3.26 (1H, dd, J=8.9, 8.0, H-2'), 3.30 (1H, ddd, J=9.2, 7.3, 5.5, H-4''), 3.31 (1H, dd, J=9.2, 7.6, H-2''), 3.32 (1H, dd, J=12.2, 7.3, H-5''a), 3.45 (1H, t, J=8.9, H-4'), 3.47 (1H, t, J=9.2, H-3''), 3.49 (1H, t, J=8.9, H-3'), 3.59 (1H, ddd, J=8.9, 5.8, 2.2, H-5'), 3.85 (1H, dd, J=11.9, 5.5, H-6'a), 3.96 (1H, dt, J=10.1, 7.0, H-8a), 3.97 (1H, dd, J=12.2, 5.5, H-5''b), 4.16 (1H, dt, J=10.1, 7.0, H-8b), 4.16 (1H, dd, J=11.9, 2.2, H-6'b), 4.46 (1H, d, J=7.6, H-1''), 4.49 (1H, d, J=8.0, H-1'), 7.31∼7.43 (5H, m, H-2'-6');13C-NMR (125 MHz, D2O) δ:38.0 (C-7), 68.0 (C-5''), 71.4 (C-6'), 72.0 (C-4''), 72.3 (C-4'), 73.7 (C-8), 75.8 (C-2'), 75.8 (C-2''), 77.7 (C-5'),78.5 (C-3'), 78.5 (C-3''), 105.0 (C-1'), 106.4 (C-1''), 129.4 (C-4), 131.5 (C-3, 5), 131.9 (C-2, 6), 141.6 (C-1).

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