Synthesis of Nanocrystalline Copper Oxide using Copper (II) Semicarbazone Derivative

Author:

K. Rana Paritosh1,Janwadkar Suhas P.1,Yadav Dilip K.1

Affiliation:

1. Department of Chemistry, S.D. Arts, V. S. Apte Commerce and M. H. Mehta, Science College, Palghar- 401404.

Abstract

The Semicarbazone derivatives of 2-4, dihydroxy acetophenone is synthesized and characterized by physico‐chemical techniques such as melting point, Ultra Violet‐Visible Spectrophotometer, Fourier Transform Infra-Red (FTIR), proton nuclear magnetic resonance (1HNMR) spectroscopy and used as a chelating agent to form complex with Copper as Copper (II) semicarbazone derivative. The synthesised Copper (II) semicarbazone complex was also studied for its complex formation IR analysis, decomposition studies using TGA. The synthesised Copper (II) semicarbazone complex was successfully employed as precursor for synthesis of nano crystalline Copper oxide and its formation was confirmed by UV-Visible spectroscopy and XRD analysis. The method successfully employed use of Copper (II) semicarbazone complex for synthesis of nano Copper oxide.

Publisher

A and V Publications

Reference20 articles.

1. Vogal A. I. ‘Text Book of qualitative Inorganic Analysis’, Longman Green and Co. ltd., London 1961.

2. L. A. Patil, D. R. Patil, Heterocontact type CuO-modified SnO2 sensor for the detection of a ppm level H2S gas at room temperature, Sens. Actuators B. 2006; 120(1): 316-323.

3. D. R. Patil, L. A. Patil, Preparation and study of NH3 gas sensing behavior of Fe2O3 doped ZnO thick film resistors, Sens. Transducers. 2006; 70(1): 661-670.

4. D. R. Patil, L. A. Patil, G. H. Jain, M. S. Wagh, S. A. Patil, Surface activated ZnO thick film resistors for LPG gas sensing, Sens. Transducers. 2006; 74(2): 874-883.

5. Khopkar S. M.; ‘Basic Concepts in Analytical Chemistry,’ 2nd edition.

Cited by 1 articles. 订阅此论文施引文献 订阅此论文施引文献,注册后可以免费订阅5篇论文的施引文献,订阅后可以查看论文全部施引文献

同舟云学术

1.学者识别学者识别

2.学术分析学术分析

3.人才评估人才评估

"同舟云学术"是以全球学者为主线,采集、加工和组织学术论文而形成的新型学术文献查询和分析系统,可以对全球学者进行文献检索和人才价值评估。用户可以通过关注某些学科领域的顶尖人物而持续追踪该领域的学科进展和研究前沿。经过近期的数据扩容,当前同舟云学术共收录了国内外主流学术期刊6万余种,收集的期刊论文及会议论文总量共计约1.5亿篇,并以每天添加12000余篇中外论文的速度递增。我们也可以为用户提供个性化、定制化的学者数据。欢迎来电咨询!咨询电话:010-8811{复制后删除}0370

www.globalauthorid.com

TOP

Copyright © 2019-2024 北京同舟云网络信息技术有限公司
京公网安备11010802033243号  京ICP备18003416号-3