A Green Protocol for Synthesis of MAl2O4, [M=Cu and Co] Spinels Under Microwave Irradiation Method-Reference-Cited by-同舟云学术

A Green Protocol for Synthesis of MAl2O4, [M=Cu and Co] Spinels Under Microwave Irradiation Method

Published:2016-09-02 Issue:03 Volume:16 Page:1650033
ISSN:0219-581X
Container-title:International Journal of Nanoscience
language:en
Short-container-title:Int. J. Nanosci.

Author:

Yuvasravana R.¹,George P. P.¹

Affiliation:

1. Department of Chemistry Madanapalle Institute of Technology and Science, (Affiliated to JNTUA, Ananthapuram and Approved by AICTE, New Delhi) Post-Box No. 14, Angallu, Madanapalle-517325, Andhra Pradesh, India

Abstract

Nanosized metal aluminates MAl2O4, [[Formula: see text] and Co] are synthesized from their nitrates solution by using pomegranate peel extract as fuel in microwave combustion. MAl2O4 [[Formula: see text] and Co] nanoparticles are grown in microwave assisted synthesis followed by annealing at 700[Formula: see text]C. The nanoparticles have been characterized by powder X-ray diffraction (PXRD), scanning electron microscopy (SEM), Fourier transform infrared spectroscopy (FTIR), UV-VIS spectroscopy and photoluminescence (PL) spectroscopy. The PXRD analysis has confirmed their spinel composition. The green protocol and microwave combustion route for spinel synthesis are rapid, simple, without any hazardous chemicals as reducing or stabilizing agents and economical.

Publisher

World Scientific Pub Co Pte Lt

Subject

Electrical and Electronic Engineering,Computer Science Applications,Condensed Matter Physics,General Materials Science,Bioengineering,Biotechnology

Link

https://www.worldscientific.com/doi/pdf/10.1142/S0219581X16500332

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