Synthesis and characterizations of peripheral octa-amino and octa-amidophthalocyanines-Reference-Cited by-同舟云学术

Synthesis and characterizations of peripheral octa-amino and octa-amidophthalocyanines

Published:2008-02 Issue:02 Volume:12 Page:123-130
ISSN:1088-4246
Container-title:Journal of Porphyrins and Phthalocyanines
language:en
Short-container-title:J. Porphyrins Phthalocyanines

Author:

Yuksel Fatma¹,Tuncel Sinem¹,Ahsen Vefa¹²

Affiliation:

1. Gebze Institute of Technology, Department of Chemistry, PO Box 141, Gebze 41400, Kocaeli, Turkey

2. TUBITAK-Marmara Research Center, Materials Institute, PO Box 21, Gebze 41470, Kocaeli, Turkey

Abstract

Novel 2,3,9,10,16,17,23,24-octaamino substituted Ni(II) phthalocyanine (2) was synthesized from tosylamido (tosyl: toluene-p-sulphonyl) derivative by the cleavage of tosyl groups in the presence of 90% sulfuric acid. Octa-hexanoylamido Ni(II) phthalocyanine (3a) and octa-lauroylamido Ni(II) phthalocyanine (3b) were obtained by reacting of octa-amino Ni(II) phthalocyanine (2) with hexanoyl chloride and lauroyl chloride, respectively. The new compounds have been characterized by elemental analysis, FT-IR, NMR and UV-vis spectroscopy and mass spectrometry. The aggregation behaviors of new compounds were investigated by UV-vis spectroscopy.

Publisher

World Scientific Pub Co Pte Lt

Subject

General Chemistry

Link

https://www.worldscientific.com/doi/pdf/10.1142/S1088424608000169

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