PREPARATION OF LUMINESCENT PbWO4 MICROCRYSTALS WITH HIERARCHICAL STRUCTURES BY USING MICROWAVE IRRADIATION HEATING METHOD

Author:

WAN GENGPING1,WANG GUIZHEN1

Affiliation:

1. College of Materials and Chemical Engineering, Key Laboratory of Ministry of Education for Application Technology of Chemical Materials in Hainan Superior Resources, Hainan University, Haikou 570228, China

Abstract

Lead tungstate ( PbWO 4) microcrystals with hierarchical structures have been successfully synthesized via a facile microwave irradiation heating method. The cetyltrimethylammonium bromine (CTAB) and microwave-heated power were found to play an important role in the morphological control of resulting PbWO 4 mirocrystals. The products were characterized by the techniques of powder X-ray diffraction and field-emission scanning electron microscopy. A growth mechanism of PbWO 4 microstructures was proposed. The luminescence properties of the final products were investigated and the as-prepared PbWO 4 microcrystals displayed a very unique room-temperature photoluminescence compared to the reported results.

Publisher

World Scientific Pub Co Pte Lt

Subject

Condensed Matter Physics,Statistical and Nonlinear Physics

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