Method for Efficient Regeneration of Solvent Mixture: Extractive Heterogeneous-Azeotropic Distillation

Author:

Tóth András József1,Schmidt Szilvia1

Affiliation:

1. BME-VBK Department of Chemical and Environmental Process Engineering, Environmental and Process Engineering Research Group , Budapest , Hungary

Abstract

Abstract The fine chemical and pharmaceutical industries use large amounts of various organic solvents in their manufacturing processes. By reusing them, production costs can be significantly reduced. If we can regenerate waste solvent mixtures, we have the opportunity to reuse them in the production process or in other production processes. Our study illustrates an efficient regeneration process using the example of a four-component solvent mixture. Calculations were performed in a professional process simulator to demonstrate that the highly non-ideal Water-Ethyl Alcohol-Methyl Ethyl Ketone-Ethyl Acetate solvent mixture can be efficiently decomposed into azeotropic pairs and thus regenerated by the extractive heterogeneous-azeotropic distillation technique.

Publisher

Muszaki Tudomanyos Kozlemenyek

Subject

General Arts and Humanities

Reference13 articles.

1. [1] Toth A. J.: Hulladékgazdálkodás a vegyiparban. Typotex, Budapest, 2020.

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3. [3] Brinkmann T., Santonja G. G., Yükseler H., Roudier S., Sancho L. D.: Best Available Techniques (BAT) Reference Document for Common Waste Water and Waste Gas Treatment/Management Systems in the Chemical Sector. Riport, Publications Office of the European Union, 2016.

4. [4] Toth A. J., Szanyi A., Koczka K., Mizsey P.: Enhanced Separation of Highly Non-Ideal Mixtures with Extractive Heterogeneous-Azeotropic Distillation. Separation Science and Technology, 51/7. (2018) 1238–1247. https://doi.org/10.1080/01496395.2015.110709910.1080/01496395.2015.1107099

5. [5] Toth A. J.: Comprehensive Evaluation and Comparison of Advanced Separation Methods on the Separation of Ethyl Acetate-Ethanol-Water Highly Non-Ideal Mixture. Separation and Purification Technology, 224. (2019) 490–508. https://doi.org/10.1016/j.seppur.2019.05.05110.1016/j.seppur.2019.05.051

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