Synthesis and X-ray crystal structure of 5β-cholan-24-yl chloride

Author:

Cox Philip J.1,Nahar Lutfun2,Turner Alan B.2

Affiliation:

1. School of Pharmacy, The Robert Gordon University, Schoolhill, Aberdeen, AB9 1FR, Scotland

2. Department of Chemistry, University of Aberdeen, Meston Walk, Old Aberdeen, AB9 2UE Scotland

Abstract

5β-cholan-24-yl chloride (5) was prepared from lithocholic acid (1) in four steps, and following spectral investigations its crystal and molecular structure was determined by X-ray crystallography.

Publisher

SAGE Publications

Subject

General Chemistry

Cited by 6 articles. 订阅此论文施引文献 订阅此论文施引文献,注册后可以免费订阅5篇论文的施引文献,订阅后可以查看论文全部施引文献

1. (20R)-24-Bromo-5β-cholane;Acta Crystallographica Section E Structure Reports Online;2009-04-25

2. Synthesis of Pregnenolone and Methyl Lithocholate Oxalate Derivatives;Natural Product Communications;2008-01

3. Synthesis of 3α-chlorinated Methyl Lithocholate Derivatives;Journal of Chemical Research;2007-02

4. Synthesis of dinorcholane and 5β-cholane derivatives;Journal of Chemical Research;2004-05

5. Synthesis of ester-linked lithocholic acid dimers;Steroids;2003-12

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