Synthesis, NMR Characterisation, X–ray Crystal Structure and Solution Studies of Ni(II) Complexes of a Pyridine Containing Self–assembling System-Reference-Cited by-同舟云学术

Synthesis, NMR Characterisation, X–ray Crystal Structure and Solution Studies of Ni(II) Complexes of a Pyridine Containing Self–assembling System

Published:2002-10 Issue:10 Volume:2002 Page:477-479
ISSN:1747-5198
Container-title:Journal of Chemical Research
language:en
Short-container-title:Journal of Chemical Research

Author:

Moghimi A.¹,Ranjbar M.²,Aghabozorg H.²,Jalali F.³,Shamsipur M.³,Chadah Raj K.⁴

Affiliation:

1. Department of Chemistry, Imam Hossein University, Tehran, Iran

2. Department of Chemistry, Teacher Training University, Tehran, Iran

3. Department of Chemistry, Razi University, Kermanshah, Iran

4. Department of Chemistry, The Scripps Research Institute, La Jolla, CA, USA

Abstract

X-ray analysis of Ni(II) complexes of the self-assembling system LH2, [pyda.H2][pydc] (pydc.H2 = 2,6-pyridinedicarboxylic acid and pyda = 2,6-pyridinediamine), indicated that two six-coordinated anionic [pyda.H]2[Ni(pydc)2].H2O (I) and neutral [Ni(pydc.H)2].3H2O (II) complexes are formed at different temperature conditions in water; in agreement with the results obtained from potentiometric pH titrations in the pH range 3.5–5.5.

Publisher

SAGE Publications

Subject

General Chemistry

Link

http://journals.sagepub.com/doi/pdf/10.3184/030823402103170646

Reference3 articles.

1. Molecular self-assembly through hydrogen bonding: supramolecular aggregates based on the cyanuric acid-melamine lattice

2. A novel pyridine containing self-assembling system: synthesis, characterization, X-ray crystal structure, 13 C solid phase NMR and solution studies

3. Design of Layered Crystalline Materials Using Coordination Chemistry and Hydrogen Bonds

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