Chlorotrimethylsilane-Promoted Synthesis of 1,2-Dihydro-1-Arylnaphtho [1,2-e] [1,3]Oxazine-3-Ones

Author:

Jiang Chenggang1,Geng Xin1,Zhang Zonglei1,Xu Hangxian1,Wang Cunde1

Affiliation:

1. College of Chemistry and Chemical Technology, Yangzhou University, Yangzhou 225002, P. R. China

Abstract

Chlorotrimethylsilane (TMSCI) is effective as a catalyst for the preparation of 1,2-dihydro-1-arylnaphtho[1,2-e] [1,3]oxazine-3- ones using a one-pot condensation of 2-naphthol, aromatic aldehydes and urea in DMF as solvent. The reaction times, temperature, and catalyst amounts were varied.

Publisher

SAGE Publications

Subject

General Chemistry

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