The Preparation and Crystal structure of 16-Acetylandrosta-4,16-Dien-3-One+

Author:

Dalmaris John1,Hanson James R.1,Hitchcock Peter B.,Kiran Ismail2

Affiliation:

1. School of Chemistry, Physics and Environmental Science, University of Sussex, Brighton, Sussex, BN1 9QJ, UK

2. Department of Chemistry, Osmangazi University, 26480, Eskışehır, Turkey

Abstract

Dehydroisoandrosterone was formylated at C-16 by a Vilsmeier reaction and by condensation with methyl formate. The product of the latter reaction was converted to 16-acetylandrosta-4,16-dien-3-one and its X-ray crystal structure was determined.

Publisher

SAGE Publications

Subject

General Chemistry

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