New Synthesis of 1,3-diaryl-4-nitro-1-butanones by Microwave-Promoted Michael Addition of Nitromethane to Chalcones without Solvent-Reference-Cited by-同舟云学术

New Synthesis of 1,3-diaryl-4-nitro-1-butanones by Microwave-Promoted Michael Addition of Nitromethane to Chalcones without Solvent

Published:2007-11 Issue:11 Volume:2007 Page:660-661
ISSN:1747-5198
Container-title:Journal of Chemical Research
language:en
Short-container-title:Journal of Chemical Research

Author:

Li Shuangshuang¹,Xie Zengyang¹,Bian Xiaoqin¹²,Wang Cunde¹

Affiliation:

1. College of Chemistry and Chemical Technology, Yangzhou University, Yangzhou 225002, P. R. China

2. Department of Environmental and Chemical Engineering, Taizhou Polytechnic College, Taizhou 225300, P. R. China

Abstract

The Michael addition of nitromethane to chalcones promoted by microwave irradiation without solvent afforded 1,3-diaryl-4-nitro-1-butanones in good yield. The products were characterised by IR, 1H NMR and elemental analysis.

Publisher

SAGE Publications

Subject

General Chemistry

Link

http://journals.sagepub.com/doi/pdf/10.3184/030823407X266199

Reference16 articles.

1. Enantioselective Michael Addition of Nitromethane to α,β-Enones Catalyzed by Chiral Quaternary Ammonium Salts. A Simple Synthesis of (R)-Baclofen

2. Synthesis of 2H-pyrroles by treatment of pyrrolidines with DDQ

3. Asymmetric hydrogenation of prochiral γ-nitroketones by ruthenium complexes

4. Enantioselective michael additions of nitromethane to α,β-unsaturated ketones catalyzed by transition metal complexes with chiral nitrogen ligands

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