Trichlorocyanuric Acid: An Efficient Reagent for One-Pot Synthesis of Ptychodiscus Brevis (PB-1) Toxin and its Derivatives-Reference-Cited by-同舟云学术

Trichlorocyanuric Acid: An Efficient Reagent for One-Pot Synthesis of Ptychodiscus Brevis (PB-1) Toxin and its Derivatives

Published:2007-01 Issue:1 Volume:2007 Page:29-33
ISSN:1747-5198
Container-title:Journal of Chemical Research
language:en
Short-container-title:Journal of Chemical Research

Author:

Gupta Arvind K.¹,Acharya Jyotiranjan¹,Dubey Devendra K.¹,Kaushik Mahabir P.¹

Affiliation:

1. Process Technology Development Division, Defence R & D Establishment, Jhansi Road, Gwalior 474002 (MP), India

Abstract

Trichlorocyanuric acid is an efficient regent for simple and one-pot synthesis of dialkyl, N-cycloctylphosphoraamidates (PB-1) and its various derivatives in excellent yields. The procedure is operationally simple and involves the reaction of various dialkylphosphites with trichloroisocyanuric acid in acetonitrile and subsequent treatment with amines in presence KF-celite to give PB-1 and derivatives.

Publisher

SAGE Publications

Subject

General Chemistry

Link

http://journals.sagepub.com/doi/pdf/10.3184/030823407780199667

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