Microwave-Assisted, Metal- and Solvent-Free Synthesis of Diaryl Thioethers from Aryl Halides and Carbon Disulfide in the Presence of [DBUH]+[OAc]−-Reference-Cited by-同舟云学术

Microwave-Assisted, Metal- and Solvent-Free Synthesis of Diaryl Thioethers from Aryl Halides and Carbon Disulfide in the Presence of [DBUH]+[OAc]−

Published:2016-05 Issue:5 Volume:40 Page:305-307
ISSN:1747-5198
Container-title:Journal of Chemical Research
language:en
Short-container-title:Journal of Chemical Research

Author:

Zhou Yongsheng¹

Affiliation:

1. School of Petrochemical Engineering, Changzhou University, Changzhou 213164, P.R. China

Abstract

A microwave-assisted direct coupling between aryl halides and carbon disulfide in ionic liquid [DBUH]+[OAc]− (DBU = 1,8-diazabicyclo-[5.4.0] undec-7-ene) has been developed. The reactions are very efficient, affording the corresponding diaryl thioethers in moderate to high yields. Aryl chlorides could also be reacted with carbon disulfide using this protocol. Moreover, [DBUH]+[OAc]− could be easily recovered and reused for several runs.

Publisher

SAGE Publications

Subject

General Chemistry

Link

http://journals.sagepub.com/doi/pdf/10.3184/174751916X14605556925623

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