Synthesis and Crystal Structure of Novel N-Acyl-2,3-Dimethyl-3,4-2H-1,4-Benzoxazine

Author:

Ye Fei1,Yang Fei1,Zhao Li-Xia1,Gao Shuang1,Fu Ying1

Affiliation:

1. College of Science, Northeast Agricultural University, Harbin, Heilongjiang 150030, P.R. China

Abstract

Novel cis-N-acyl-2,3-dimethyl-3,4-2H-1,4-benzoxazine derivatives were synthesised by acylation of 2,3-dimethyl-3,4-dihydro-2H-1,4-benzoxazine derivatives, which were prepared via the reduction and cyclisation of 3-(o-nitrophenoxy)butan-2-one. The configuration was determined by X-ray crystallography.

Publisher

SAGE Publications

Subject

General Chemistry

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