Determination of Pentachlorophenol in Blood, Urine, Tissue, and Clothing

Author:

Barth W F1,Curley August1,Thrasher C L1,Sedlak V A1,Armstrong Robert2

Affiliation:

1. Toxicology Laboratory, Pesticides Program, Food and Drug Administration, Consumer Protection and Environmental Health Service, Atlanta, Ga. 30333

2. Epidemiology Program, National Communicable Disease Center, Public Health Service, Atlanta, Ga. 30333

Abstract

Abstract An epidemic with two deaths occurred in a nursery in St. Louis after the use of pentachlorophenol as a mildew preventive with the laundry detergent. Samples of blood, urine, tissue, and clothing from the nursery were extracted with ethyl ether. The ether solution was extracted with 5% sodium hydroxide; the basic solution was acidified and then extracted with benzene. The benzene solution was analyzed by electron capture gas chromatography, using a 3% diethylene glycol succinate column with 2% sirupy phosphoric acid on 60-80 mesh Chromosorb G. Pentachlorophenol was found in the samples in sufficient quantity to account for the epidemic. The presence of pentachlorophenol was confirmed by gas chromatogrifplryrmass spectroscopy and by thin layer analysis.

Publisher

Oxford University Press (OUP)

Subject

General Chemistry

Cited by 3 articles. 订阅此论文施引文献 订阅此论文施引文献,注册后可以免费订阅5篇论文的施引文献,订阅后可以查看论文全部施引文献

1. A method for extraction of pentachlorophenol from plant tissues;Zeitschrift für Pflanzenernährung und Bodenkunde;1991-01

2. Determination of Pentachlorophenol Laurate by High Pressure Liquid Chromatography;Journal of Liquid Chromatography;1981-01

3. Metabolism of pentachlorophenol;Archives of Toxicology;1974

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