Evaluation of depth of dislocation visibility in SEM electron channeling contrast imaging in Ti-6Al-4V alloy using serial sectioning method

Author:

Yamasaki Shigeto1,Deguchi Misaki2,Mitsuhara Masatoshi3,Nakashima Hideharu3,Ota Yutaro4,Kubushiro Keiji5

Affiliation:

1. Department of Materials Science and Engineering, Kyushu University, Fukuoka, Fukuoka 819-0395, Japan

2. Interdisciplinary Graduate School of Engineering Sciences, Kyushu University, Kasuga, Fukuoka 819-0395, Japan

3. Department of Advanced Materials Science, Kyushu University, Kasuga, Fukuoka 816-8580, Japan

4. Metals & Materials Evaluation Group, Technology Platform Center, IHI Corporation, Yokohama, Kanagawa 235-8501, Japan

5. Data & Service Center, IHI ASIA PACIFIC (Thailand) Co., Ltd., Bang Rak, Bangkok 10500, Thailand

Abstract

Abstract In this study, we conducted a quantitative evaluation of dislocation density by scanning electron microscopy electron channeling contrast imaging for α grains of a Ti-6Al-4V alloy deformed at room temperature. The depth of visibility of dislocations is experimentally measured as 140 to 160 nm by a serial sectioning observation. This result is compared with the theoretical value and applied to evaluate dislocation density. These factors confirm that the theoretically calculated value of the depth of visibility, at 5 to 6 times the extinction distance, is valid for the hexagonal close-packed Ti alloy.

Funder

IHI Corporation

Publisher

Oxford University Press (OUP)

Subject

Radiology, Nuclear Medicine and imaging,Instrumentation,Structural Biology

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