Determination of Maduramicin in Feedingstuffs and Premixtures by Liquid Chromatography: Development, Validation, and Interlaboratory Study

Author:

Jong Jacob De1,Stoisser Bernd2,Wagner Karl2,Tomassen Marinka3,Driessen Jaap3,Hofmann Peter1,Putzka Hans-Artur4,Antalick J P,Cowles J,Felgueiras I,Hofmann P,Johannsen F H,Putzka H A,Stepinska A,Stoisser; B,Thalmann A,van der Kamp H J,van Schalm K,

Affiliation:

1. RIKILT-Institute of Food Safety, PO Box 230, 6700 AE, Wageningen, The Netherlands

2. Austrian Agency for Health and Food Safety, Agricultural Inspection Service and Research Centre Vienna (AGES-LWVIE), Spargelfeldstraße 191, A-1226 Vienna, Austria

3. Hoffmann-La Roche Ltd., Bau 71/248, CH-4070, Basel, Switzerland

4. Universität Hamburg, Institut für Angewandte Botanik, PO Box 302762, D-20309, Hamburg, Germany

Abstract

Abstract A reversed-phase liquid chromatography method for determination of maduramicin in feedingstuffs and premixtures was developed, validated, and interlaboratory studied. The extraction solvent was methanol. Maduramicin was detected at 520 nm after postcolumn derivatization with vanillin.

Publisher

Oxford University Press (OUP)

Subject

Pharmacology,Agronomy and Crop Science,Environmental Chemistry,Food Science,Analytical Chemistry

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