1. Agriculture and the Environment Division; Rothamsted Research; Harpenden Herts AL5 2JQ UK
2. Dep. of Chemistry, Queen Mary; Univ. of London; London E1 4NS UK
3. Embrapa Solos; Rua Jardim Botanico 1024 22460-000 Rio de Janeiro RJ Brazil
4. Dep. of Earth, Atmospheric, and Planetary Sciences; Massachusetts Institute of Technology; 77 Massachusetts Ave. Cambridge MA 02139