Densification Study of SiC:Al2O3:Y2O3 with Polymer Additions

Author:

Godoy Ana Lúcia Exner1,Bressiani José Carlos2,Bressiani Ana Helena A.3

Affiliation:

1. Instituto de Pesquisas Energéticas e Nucleares, IPEN

2. Instituto de Pesquisas Energeticas e Nucleares

3. IPEN/CNEN, Instituto de Pesquisas Energéticas e Nucleares

Abstract

The influence of polymer precursor additions on liquid phase sintering of SiC:Al2O3:Y2O3 has been evaluated. Two polymer precursors were used: polymethylhydrogensiloxane and D4Vi (1,3,5,7-tetramethyl-1,3,5,7-tetraviniylcyclotetrasiloxane). The ceramic phase had the following composition in wt%: 91.6 SiC, 4.2 Al2O3 and 4.2 Y2O3. The composites were prepared using the following ceramic phase to polymer ratios in wt%: 82.7: 17.3; 74.0: 26.0 and 71.5: 28.5. Density measurements were carried out using a helium picnometry and the Archimedes method. The crystalline phases were identified by X-ray diffraction analysis and the microstructures were observed by optical and scanning electron microscopy.

Publisher

Trans Tech Publications, Ltd.

Subject

Mechanical Engineering,Mechanics of Materials,Condensed Matter Physics,General Materials Science

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