Consolidation of Aluminium Oxynitride Powders Using Hydrolysis of Aluminium Nitride

Author:

Bućko Mirosław M.1,Domagała Jakub1,Lach Radosław1

Affiliation:

1. AGH - University of Science and Technology

Abstract

One of the materials with high potential for application as a refractory material is aluminum oxynitride with spinel-type structure, γ-alon. Alon materials, single-phase or composites, are characterized by good mechanical properties, high thermal shock resistance and a high corrosion and erosion resistance. Another advantage is possibility of usage of SHS method for producing of relatively good sinterable powders of γ-alon, however, are characterized by poor compressibility. This paper describes a method of compaction of SHS-derived γ-alon powder using the hydrolysis reaction of aluminum nitride, which is one of the products of SHS synthesis. The green bodies made from the powder with addition of 10 mas.% of water after two weeks of storage reach a strength level up to 30 MPa and an open porosity of less than 30%. Pressureless sintering of the such compacts allows to achieve 95% of theoretical density at 1700°C in less than one minute.

Publisher

Trans Tech Publications, Ltd.

Subject

Mechanical Engineering,Mechanics of Materials,General Materials Science

Reference7 articles.

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3. D. Launay, G. Orange, P. Goeuriot, F. Thevenot, G. Fantozzi, Reaction-sintering of an Al2O3–ALON composite determination of mechanical properties, J. Mater. Sci. Lett. 3 (1984) 890-892.

4. J. Domagała, D. Zientara, P. Rutkowski, G. Grabowski, J. Lis, Manufacturing and properties of materials from the corundum/ γ-alon system, Materiały Ceramiczne/Ceramic Materials 63 (2011) 802-808.

5. D. Zientara, M. Bućko, J. Lis, Aluminium oxynitride as a crucible material for melting of nickel-based superalloys, in: J.G. Heinrich, C.G. Aneziris (Eds. ), Proceedings of the 10th International Conference of the European Ceramic Society, Göller Verlag, Baden-Baden, 2007, pp.1882-1885.

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