Affiliation:
1. Kunming University of Science and Technology
2. Wuhan University
Abstract
A neotype of silica microspheres were synthesized with chloropropyltrimethoxysilane (WD30) and tetraethoxysilane (TEOS) by sol-gel method. And the thermal properties of the filler both in nitrogen and in air condition were studied by means of thermogravimetric analysis. The morphology of the filler was measured by TEM. The so synthesized spheres were added into the silicone rubber whose mechanical strength was increased greatly. The molecular structure of the filler and the silicone rubber were characterized by FTIR. The possible strengthen mechanism of the filler was discussed. The neotype silica sphere researched in this paper could react with the PDMS chains which perfects the vulcanization of the silicone rubber. This kind of silica sphere exhibits many merits for usage as filler.
Publisher
Trans Tech Publications, Ltd.