Cascaded Columns of Total Reflux Batch Distillation with Periodic Liquid Exchange

Author:

Tang Ke1,Bai Peng1

Affiliation:

1. Tianjin University

Abstract

A new type of operation mode of cascaded columns of total reflux batch distillation with periodic liquid exchange was proposed. The feasibility of the new operation, which is suitable for separations of mixtures of close boiling point, thermo-sensitive material and isotopes, was proved by the experiments in which two columns and three columns in periodic liquid exchange were used with ethanol-isopropanol, ethylbenzene- paraxylene as the experimental mixtures. The results indicate that the new operation mode can generate summation effect of theoretical plates by periodic liquid exchange between columns, while the total pressure drop is the same as that of a single column.

Publisher

Trans Tech Publications, Ltd.

Subject

General Engineering

Reference7 articles.

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2. Yang, Z. C., Batch distillation process in Chemical Industry— principle, technology and equipments, Chemical Industry Press, Bei Jing (2001).

3. Han, L. G., J. Y. Yu, and W. J. Zhang, Advance in industry separation technology of abundant boron isotopes, Isotopes, China, vol. 19, iss. 1, p.48–52 (2006).

4. PALKO A. A., J. S. DRURY, Separation of boron isotopes. Ⅵ. Ethylether , ethyl sulfide , and triethylamine-BF3systems, Chem. Phys., vol. 40, iss. 2, p.278– 281 (1964).

5. SEVRYUGOVA, N, N., UVAROV O V, Separation of the stable isotopes of boron, Atomic Energy, vol. 29, iss. 2, p.614 – 629, (1961).

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