Synthesis of Diamine Containing Chalcone Structure by Nitroammoniation and Aldol Condensation-Reference-Cited by-同舟云学术

Synthesis of Diamine Containing Chalcone Structure by Nitroammoniation and Aldol Condensation

Published:2019-05 Issue: Volume:801 Page:145-150
ISSN:1662-9795
Container-title:Key Engineering Materials
language:
Short-container-title:KEM

Author:

Huang Yan Kai¹,Mei Qi Lin¹,Huang Zhi Xiong¹,Qin Yan¹,Zhu Di¹

Affiliation:

1. Wuhan University of Technology

Abstract

In this paper, the structure of the photosensitive diamines was designed and the method of synthesizing such diamines was investigated. The 1-(3-aminophenyl)-3-(4-aminophenyl)-2-propen-1-one analyzed by elemental analysis and infrared analysis was synthesized through two-step experiments with Aldol condensation and Nitroammoniation process. Through the experiment the optimum reaction conditions are raw material ratio of 1:1, anhydrous ethanol dosage of 60 ml, 10 % NaOH dosage of 10 ml and reaction temperature of 25°C for 4h. The yield was about 55.4 %.

Publisher

Trans Tech Publications, Ltd.

Subject

Mechanical Engineering,Mechanics of Materials,General Materials Science

Link

https://www.scientific.net/KEM.801.145.pdf

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