Redetermination of the Niobium(V) Precursor, [NbCl5(NCCH3)]

Author:

Herbst Leandra1,Visser Hendrik G.1,Roodt Andreas1

Affiliation:

1. University of the Free State

Abstract

The monomeric coordination compound pentachloro(acetonitrile)niobium(V), [NbCl5(NCCH3)], (NCCH3= acetonitrile) has been prepared under aerobic conditions and characterized by single-crystal X-ray diffraction. [NbCl5(NCCH3)] crystallized in the monoclinic spacegroupP21/cwitha= 5.964 (3),b= 9.888 (5),c= 15.448 (9) and β = 98.224 (2). Comparison is made to a previously published isomorphous complex that was prepared under unaerobic conditions.

Publisher

Trans Tech Publications, Ltd.

Subject

General Engineering

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