Preparation and Characterization of Gamma Radiation Cured Gelatin-PVA Bio-Blend

Author:

Khan Mubarak A.1,Rahman Nazia1,Rahman M.1

Affiliation:

1. Bangladesh Atomic Energy Commission

Abstract

Gelatin-PVA blend films of different compositions (0%, 5%, 10%, 15% of PVA) were prepared by casting. The tensile strength (TS) and elongation at break (Eb) of the films were studied. The TS and Eb of pure gelatin films were found to be 32 MPa and 3.3% respectively. The films were irradiated under different gamma radiation dose (50 Krad, 100 Krad, 150 Krad, 250 Krad, 500 Krad). 5% PVA containing gelatin films irradiated under 100 Krad gamma radiation showed highest TS of 42 MPa and highest Eb of 4.2%. Thermal property of the films was studied by Thermomechanical analysis (TMA) and Thermogravimetric Analysis (TGA). The grafting of PVA onto gelatin is studied by IR. In order to study surface morphology SEM study was undertaken.

Publisher

Trans Tech Publications, Ltd.

Subject

General Engineering

Reference5 articles.

1. J.E. Eastoe, A. A. Leach: Recent advance in gelatin and Glue research (Pergamon press, New York 1958).

2. National formulary XVI, United States Pharmacopial convention, Inc., Rockville, Maryland 1984, pp.1563-1564.

3. International Agency for Research on Cancer (IARC) ; Lyon, France. IARC monographs on the Evaluation of the Carcinogenic Risk of Chemicals to man, Vol. 19 (1978), p.341.

4. Kashi Sasaki, Radiation Polymerization, UNDP/IAEA/RCA Regional Training Course on Radiation Chemistry, JAERI, Vol. 19 (1991), pp.1-12.

5. Kaetsu I : Radiat. Phys. Chem. Vol. 25 (1985), p.517. Figure 5: A SEM micrograph of untreated gelatin film Figure 6: A SEM micrograph of radiated film (95%PVA+5%gelatin).

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