Preparation and Characterization of Cubic and Rod-Shaped Indium Tin Oxide Powders Using the Hydrothermal Process

Author:

Hsu Kuo Chin1,Liao Jiunn Der1,Xie Zheng Zhong1,Fu Yaw Shyan2

Affiliation:

1. National Cheng Kung University

2. National University of Tainan

Abstract

The cubic and rod-shaped powders of indium tin oxide were synthesized at a stable temperature reaction for 18h using the surfactant aid hydrothermal method under various conditions. The cubic and rod-shaped powder size changes with the concentration of the precursor. The finished products of indium tin oxide can be obtained by calcination at 500°C for 2h in air. Characterization was conducted using scanning electron microscopy (SEM), energy dispersive spectrometry (EDS), X-ray diffractometry (XRD), thermogravimetric analyzer/differential thermal analysis (TG/DTA) and the Brunauer-Emmett-Teller (BET). XRD analysis shows that the conditions of this experiment can produce pure ITO powders. The characterization of cubic and rod-shaped ITO powders is also discussed.

Publisher

Trans Tech Publications, Ltd.

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