Abstract
A novel Ni metal complex H26Mo6N2NiO30has been synthesized from hydrothermal reaction and the crystal structure has been determined by means of single-crystal X-ray diffraction. H26Mo6N2NiO30, Monoclinic, P2(1)/c. a = 11.3487(14) Å, b = 11.0823(13) Å, c = 11.9350(16) Å. alpha=gamma= 90°. beta= 108.542(2)°. V= 1423.1(3) Å3. It is also striking that the structure of title compound exhibits extensive hydrogen-bonding interactions among water molecules, ammonium cation, and oxygen atoms in the heteropolyanion.
Publisher
Trans Tech Publications, Ltd.