Two-Dimensional X-Ray Diffraction for Structure and Stress Analysis

Author:

He Bob B.1,Xu Ke Wei2,Wang Fei3,Huang Ping3

Affiliation:

1. Bruker AXS Incorporation

2. Xi’an University of Arts and Science

3. Xi'an Jiaotong University

Abstract

This paper introduces the recent progress in two-dimensional X-ray diffraction as well as its applications in microstructure and residual stress analysis. Based on the matrix transformation between diffraction space, detector space and sample space, the unit vector of the diffraction vector can be expressed in the sample space corresponding to all the geometric parameters and Bragg conditions. The same transformation matrix can be used for texture and stress analysis. The fundamental equations for both stress measurement and texture measurement are developed with the matrix transformation defined for the two-dimensional diffraction. Stress measurement using twodimensional detector is based on a direct relationship between the stress tensor and the diffraction cone distortion. The two-dimensional detector collects texture data and background values simultaneously for multiple poles and multiple directions.

Publisher

Trans Tech Publications, Ltd.

Subject

Mechanical Engineering,Mechanics of Materials,Condensed Matter Physics,General Materials Science

Reference9 articles.

1. P. R. Rudolf and B. G. Landes, Two-dimensional X-ray Diffraction and Scattering of Microcrystalline and Polymeric Materials, Spectroscopy, 9(6), Jul/Aug (1994), pp.22-33.

2. S. N. Sulyanov, A. N. Popov and D. M. Kheiker, Using a Two-dimensional Detector for X-ray Powder Diffractometry, J. Appl. Cryst. 27 (1994), pp.934-942.

3. B. B. He, U. Preckwinkel and K. L. Smith, Fundamentals of two-dimensional x-ray diffraction (XRD2), Advances in X-ray Analysis, Vol. 43, the 48th Annual Denver X-ray Conference, Steamboat Springs, Colorado, USA (1999).

4. Bob B. He, Introduction to two-dimensional X-ray diffraction, Powder Diffraction, Vol. 18, No 2, June (2003).

5. B. B. He, U. Preckwinkel and K. L. Smith, Advantages of Using 2D Detectors for Residual Stress Measurements, Advances in X-ray Analysis, Vol. 42, the 47th Annual Denver X-ray Conference, Colorado Springs, USA (1998).

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