Affiliation:
1. Northeastern University
Abstract
High-purity and homogeneous powders of CeB6 with nanometer size were prepared by combustion synthesis and subsequent acid- leaching. The effects of reactant ratio on the phase and morphology of the combustion product were discussed. The combustion product and leached product were analyzed by XRD, SEM and EDS. The results indicate that the combustion product consists of CeB6, MgO and Mg3B2O6. The combustion products are denser and less layered when the Mg content and KClO3 content increase. The content of CeB6 in the combustion product could be enhanced with increasing the excessive content of Mg. The purity of CeB6 is higher than 99.0% and its particles are smaller than 150nm.
Publisher
Trans Tech Publications, Ltd.
Reference13 articles.
1. Balakrishnan G, Lees M R, McK Paul D, et al. Journal of Crystal Growth, Vol 256(1/2) (2003),: p.206.
2. Zou Chun Yun, Zhao Yan Ming, Xu Jun Qi, et al. Journal of Crystal Growth, Vol291(1)( 2006), p.112.
3. Togawaa K, Babaa H, Onoea K, et al. Nuclear Instruments and Methods in Physics Research A, Vol 528(4)(2004), p.312.
4. Otani S, Nakagawa H, Nishi Y, et al. Journal of Solid State Chemistry, Vol 154(1) (2009), p.238.
5. ZHANG Ting-an, DOU Zhi-he. Journal of Northeastern University (Natural Science), Vol 25(1)(2004), p.271, In Chinese.
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